| Course label : | Experimental analytical chemistry |
|---|---|
| Teaching departement : | CMA / |
| Teaching manager : | Madam CAROLINE PIROVANO |
| Education language : | |
| Potential ects : | 0.0 |
| Results grid : | |
| Code and label (hp) : | ENSCL_CI_M5_1_2 - Spectro. moléculaires appliq. |
Education team
Teachers : Madam CAROLINE PIROVANO / Madam CHARLOTTE BECQUART / Madam FABIENNE SAMYN / Mister ERIC BUISINE / Mister LUDOVIC THUINET / Mister MOHAMED TAIEB BAKOUCHE
External contributors (business, research, secondary education): various temporary teachers
Summary
Practical work in analytical chemistry begins with an introduction to the basic techniques of the laboratory: weighing, calibration of calibrated glassware, basics of titration, and implementation of an analysis compatible with a desired precision (1 tutorial and 1 practical training session followed by an evaluation session). In this cycle of manipulations are then approached: - Water hardness determination; - Acid-base titrations by pHmetry and conductimetry; - The simulation of pH-metric dosage curves; - Anion determination by potentiometry and ion chromatography; - Voltammetric analysis; - Atomic spectroscopy analyses.
Educational goals
Following this practical training, students should be able to: - Be able to execute experimental techniques to carry out qualitative or quantitative analyses; - Implement and validate of methods for basic analytical techniques; - Analyse, exploit and discuss experimental data; - Know how to integrate the concept of measurement uncertainties and to estimate them; - Write experimental reports; - Use computer tools to exploit results and/or pilot analytical methods; - Follow Good Laboratory Practice (GLP); - Follow health and safety guidelines.
Sustainable development goals
Knowledge control procedures
Continuous Assessment
Comments: For each session, restitution in different possible formats (result sheet, brief report, report, etc.). The overall mark for each practical covers: behaviour in the laboratory room (involvement, handling, GLP, etc.), answers to questions during the session, and the restitution work.
Online resources
Practical workbook and booklet for assistance in estimating the uncertainties of the measurements are provided. Presentation support "Safety and GLP in the practical work rooms" and preparatory tutorial are available on the intranet as well as the results sheets useful for the preparation of the practical sessions.
Pedagogy
Individual or group practical work. Discovery laboratory training (new analysis techniques) and/or application laboratory training (understanding of phenomena and physico-chemical laws through experimental implementation).
Sequencing / learning methods
| Number of hours - Lectures : | 3 |
|---|---|
| Number of hours - Tutorial : | 0 |
| Number of hours - Practical work : | 7 |
| Number of hours - Seminar : | 0 |
| Number of hours - Half-group seminar : | 0 |
| Number of student hours in TEA (Autonomous learning) : | 0 |
| Number of student hours in TNE (Non-supervised activities) : | 0 |
| Number of hours in CB (Fixed exams) : | 0 |
| Number of student hours in PER (Personal work) : | 0 |
| Number of hours - Projects : | 0 |
Prerequisites
Bases acquired in preparatory years. Knowledge of health and safety measures in the laboratory.