| Course label : | Applied molecular spectroscopy |
|---|---|
| Teaching departement : | CMA / |
| Teaching manager : | Mister ERIC BUISINE |
| Education language : | |
| Potential ects : | 0 |
| Results grid : | |
| Code and label (hp) : | ENSCL_CI_M7_1_4_1 - Spectro. molécul. appliquées |
Education team
Teachers : Mister ERIC BUISINE / Madam MELISSANDRE RICHARD / Mister PHILIPPE COTELLE
External contributors (business, research, secondary education): various temporary teachers
Summary
This course (Lectures 6h and Tutorials 16h) is divided into 2 parts: A/ 14 hours dedicated to the teaching of chromatography techniques (gas and liquid) coupled with mass spectrometry. B/ Tutorials (8 hours) dedicated to the processing and analysis of one-dimensional (1D) and two-dimensional (2D) NMR spectroscopy signals and spectra.
Educational goals
A/ About chromatographic techniques: - The goal is to acquire both theoretical and practical knowledge of analytical techniques widely used in the chemical industry: Operating principle and associated theories, choice of instruments (injectors, columns, detectors, etc.) and methods. - At the end of this module, the student will be able to: - explain the principles/fundamental concepts of the different techniques, - identify chemical phenomena involved in the separation process and the parameters influencing them, - choose the right conditions (instruments and methods) for a good chromatographic separation, - process the results and verify their quality. B/ For NMR tutorials: - Knowledge: The main 1D and 2D NMR experiments necessary for the structural elucidation of small organic molecules (their principles and the information they provide). - Skills: - Choice of the most suitable 1D and 2D NMR experiments in order to elucidate the structure of the studied molecule, - Processing of 1D NMR signals obtained for 1H and 13C nuclei and 2D homonuclear 1H-1H and heteronuclear 1H-13C signals: apodization, Fourier transform, phase correction, baseline correction, calibration, - Analysis and exploitation of 1D and 2D NMR spectra: integration, signal attribution, correlation peak attribution, chemical shift measurement, fine structure analysis, measurement of coupling constants of 1st order fine structures, - Estimation of measurement accuracy, presentation of measurement results.
Sustainable development goals
Knowledge control procedures
Continuous Assessment
Comments: A/ Written test 1h30
B/ The evaluation of knowledge and skills will be done during practical teaching ENSCL_CI2021_C7_1_5
Online resources
Pedagogy
A large part of the module is dedicated to case studies / analysis of results in small groups during tutorials. The theoretical part is enhanced with examples, mini-MCQs, videos etc. to help understanding and control knowledge.
Sequencing / learning methods
| Number of hours - Lectures : | 7 |
|---|---|
| Number of hours - Tutorial : | 16 |
| Number of hours - Practical work : | 0 |
| Number of hours - Seminar : | 0 |
| Number of hours - Half-group seminar : | 0 |
| Number of student hours in TEA (Autonomous learning) : | 0 |
| Number of student hours in TNE (Non-supervised activities) : | 0 |
| Number of hours in CB (Fixed exams) : | 0 |
| Number of student hours in PER (Personal work) : | 0 |
| Number of hours - Projects : | 0 |
Prerequisites
A/ Basics of Chemistry. B/ First-year teaching ofￜ Applied Molecular Spectroscopy ￜ (ENSCL_CI2021_C5_2_2).